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EPU (ThermoFisher Scientific) was used to automate data collection which involved implementing beam-tilt to collect a 3 3 grid of holes

[DOI] [PubMed] [Google Scholar] Skibicka, K

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If you still do not think you received the full dose, do not start over or repeat the injection

Cooled the reaction mixture to 0-5 C, water (300 ml) was slowly added to it and stirred for 15 min at the same temperature

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